PoplarV1, Main, Exploration, bibRecord, 000F63

Development of supercritical CO2 extraction of bioactive phytochemicals from black poplar (Populus nigra L.) buds followed by GC-MS and UHPLC-DAD-QqTOF-MS.

Identifieur interne : 000F63 ( Main/Exploration ); précédent : 000F62; suivant : 000F64

Development of supercritical CO2 extraction of bioactive phytochemicals from black poplar (Populus nigra L.) buds followed by GC-MS and UHPLC-DAD-QqTOF-MS.

Auteurs : Piotr M. Ku [Pologne] ; Piotr Oki Czyc [Pologne] ; Martina Jakovljevi [Croatie] ; Stela Joki [Croatie] ; Igor Jerkovi [Croatie]

Source :

Journal of pharmaceutical and biomedical analysis [ 1873-264X ] ; 2018.

RBID : pubmed:29852355

Descripteurs français

English descriptors

KwdEn :
- Carbon Dioxide (chemistry), Chemical Fractionation (instrumentation), Chemical Fractionation (methods), Chromatography, High Pressure Liquid (instrumentation), Chromatography, High Pressure Liquid (methods), Flavonoids (isolation & purification), Flavonoids (pharmacology), Gas Chromatography-Mass Spectrometry (instrumentation), Gas Chromatography-Mass Spectrometry (methods), Green Chemistry Technology (instrumentation), Green Chemistry Technology (methods), Plant Extracts (chemistry), Plant Extracts (pharmacology), Populus (chemistry), Sesquiterpenes (isolation & purification), Sesquiterpenes (pharmacology), Temperature (MeSH).
MESH :
- chemical , chemistry : Carbon Dioxide, Plant Extracts.
- chemistry : Populus.
- instrumentation : Chemical Fractionation, Chromatography, High Pressure Liquid, Gas Chromatography-Mass Spectrometry, Green Chemistry Technology.
- chemical , isolation & purification : Flavonoids, Sesquiterpenes.
- methods : Chemical Fractionation, Chromatography, High Pressure Liquid, Gas Chromatography-Mass Spectrometry, Green Chemistry Technology.
- chemical , pharmacology : Flavonoids, Plant Extracts, Sesquiterpenes.
- Temperature.

Abstract

The supercritical CO₂ (SC-CO₂) extraction process of black poplar (Populus nigra L.) buds was optimized (pressure, temperature) based on the yields of major phytochemicals (volatiles and non-volatiles). The optimal settings were 30 MPa/60 °C. Major volatiles determined by GC-MS in the optimized SC-CO₂ extract (mg of benzyl salicylate equivalent (BSE) per 100 g of buds) were: pinostrobin chalcone (1574.2), β-eudesmol (640.8), α-eudesmol (581.9), 2-methyl-2-butenyl-p-coumarate (289.9), pentyl-p-coumarate (457.0), γ-eudesmol (294.4), and benzyl salicylate (289.2). Partial qualitative similarity was observed between SC-CO₂ extracts and corresponding hydrodistilled essential oil dominated by sesquiterpenes, but with lower yields. Major compounds (mg per 100 g of buds) identified by UHPLC-DAD-QqTOF-MS in the optimized SC-CO₂ extract were: pinostrobin (751.7), pinocembrin (485.6), 3-O-pinobanksin acetate and methyl-butenyl-p-coumarate (290.2; 144.9 of pinobanksin and p-coumaric acid equivalents, respectively). SC-CO₂ extraction was found useful for green, efficient and simultaneous extraction of both volatile/non-volatile, bioactive phytochemicals of poplar buds - precursors of poplar-type propolis.

DOI: 10.1016/j.jpba.2018.05.041
PubMed: 29852355

Affiliations:

Croatie, Pologne

Links toward previous steps (curation, corpus...)

to stream Main, to step Corpus: 000E05
to stream Main, to step Curation: 000E05

Le document en format XML

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 extraction of bioactive phytochemicals from black poplar (Populus nigra L.) buds followed by GC-MS and UHPLC-DAD-QqTOF-MS.</title>
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 extraction of bioactive phytochemicals from black poplar (Populus nigra L.) buds followed by GC-MS and UHPLC-DAD-QqTOF-MS.</title>
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<term>Chemical Fractionation (instrumentation)</term>
<term>Chemical Fractionation (methods)</term>
<term>Chromatography, High Pressure Liquid (instrumentation)</term>
<term>Chromatography, High Pressure Liquid (methods)</term>
<term>Flavonoids (isolation & purification)</term>
<term>Flavonoids (pharmacology)</term>
<term>Gas Chromatography-Mass Spectrometry (instrumentation)</term>
<term>Gas Chromatography-Mass Spectrometry (methods)</term>
<term>Green Chemistry Technology (instrumentation)</term>
<term>Green Chemistry Technology (methods)</term>
<term>Plant Extracts (chemistry)</term>
<term>Plant Extracts (pharmacology)</term>
<term>Populus (chemistry)</term>
<term>Sesquiterpenes (isolation & purification)</term>
<term>Sesquiterpenes (pharmacology)</term>
<term>Temperature (MeSH)</term>
</keywords>
<keywords scheme="KwdFr" xml:lang="fr"><term>Chromatographie en phase liquide à haute performance (instrumentation)</term>
<term>Chromatographie en phase liquide à haute performance (méthodes)</term>
<term>Chromatographie gazeuse-spectrométrie de masse (instrumentation)</term>
<term>Chromatographie gazeuse-spectrométrie de masse (méthodes)</term>
<term>Dioxyde de carbone (composition chimique)</term>
<term>Extraits de plantes (composition chimique)</term>
<term>Extraits de plantes (pharmacologie)</term>
<term>Flavonoïdes (isolement et purification)</term>
<term>Flavonoïdes (pharmacologie)</term>
<term>Fractionnement chimique (instrumentation)</term>
<term>Fractionnement chimique (méthodes)</term>
<term>Populus (composition chimique)</term>
<term>Sesquiterpènes (isolement et purification)</term>
<term>Sesquiterpènes (pharmacologie)</term>
<term>Technologie de la chimie verte (instrumentation)</term>
<term>Technologie de la chimie verte (méthodes)</term>
<term>Température (MeSH)</term>
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<term>Plant Extracts</term>
</keywords>
<keywords scheme="MESH" qualifier="chemistry" xml:lang="en"><term>Populus</term>
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<term>Extraits de plantes</term>
<term>Populus</term>
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<term>Chromatography, High Pressure Liquid</term>
<term>Gas Chromatography-Mass Spectrometry</term>
<term>Green Chemistry Technology</term>
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<term>Sesquiterpenes</term>
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<keywords scheme="MESH" qualifier="isolement et purification" xml:lang="fr"><term>Flavonoïdes</term>
<term>Sesquiterpènes</term>
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<keywords scheme="MESH" qualifier="methods" xml:lang="en"><term>Chemical Fractionation</term>
<term>Chromatography, High Pressure Liquid</term>
<term>Gas Chromatography-Mass Spectrometry</term>
<term>Green Chemistry Technology</term>
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<keywords scheme="MESH" qualifier="méthodes" xml:lang="fr"><term>Chromatographie en phase liquide à haute performance</term>
<term>Chromatographie gazeuse-spectrométrie de masse</term>
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<term>Technologie de la chimie verte</term>
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<term>Flavonoïdes</term>
<term>Sesquiterpènes</term>
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<front><div type="abstract" xml:lang="en">The supercritical CO<sub>2</sub>
 (SC-CO<sub>2</sub>
) extraction process of black poplar (Populus nigra L.) buds was optimized (pressure, temperature) based on the yields of major phytochemicals (volatiles and non-volatiles). The optimal settings were 30 MPa/60 °C. Major volatiles determined by GC-MS in the optimized SC-CO<sub>2</sub>
 extract (mg of benzyl salicylate equivalent (BSE) per 100 g of buds) were: pinostrobin chalcone (1574.2), β-eudesmol (640.8), α-eudesmol (581.9), 2-methyl-2-butenyl-p-coumarate (289.9), pentyl-p-coumarate (457.0), γ-eudesmol (294.4), and benzyl salicylate (289.2). Partial qualitative similarity was observed between SC-CO<sub>2</sub>
 extracts and corresponding hydrodistilled essential oil dominated by sesquiterpenes, but with lower yields. Major compounds (mg per 100 g of buds) identified by UHPLC-DAD-QqTOF-MS in the optimized SC-CO<sub>2</sub>
 extract were: pinostrobin (751.7), pinocembrin (485.6), 3-O-pinobanksin acetate and methyl-butenyl-p-coumarate (290.2; 144.9 of pinobanksin and p-coumaric acid equivalents, respectively). SC-CO<sub>2</sub>
 extraction was found useful for green, efficient and simultaneous extraction of both volatile/non-volatile, bioactive phytochemicals of poplar buds - precursors of poplar-type propolis.</div>
</front>
</TEI>
<pubmed><MedlineCitation Status="MEDLINE" Owner="NLM"><PMID Version="1">29852355</PMID>
<DateCompleted><Year>2018</Year>
<Month>11</Month>
<Day>05</Day>
</DateCompleted>
<DateRevised><Year>2018</Year>
<Month>11</Month>
<Day>05</Day>
</DateRevised>
<Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1873-264X</ISSN>
<JournalIssue CitedMedium="Internet"><Volume>158</Volume>
<PubDate><Year>2018</Year>
<Month>Sep</Month>
<Day>05</Day>
</PubDate>
</JournalIssue>
<Title>Journal of pharmaceutical and biomedical analysis</Title>
<ISOAbbreviation>J Pharm Biomed Anal</ISOAbbreviation>
</Journal>
<ArticleTitle>Development of supercritical CO<sub>2</sub>
 extraction of bioactive phytochemicals from black poplar (Populus nigra L.) buds followed by GC-MS and UHPLC-DAD-QqTOF-MS.</ArticleTitle>
<Pagination><MedlinePgn>15-27</MedlinePgn>
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<Abstract><AbstractText>The supercritical CO<sub>2</sub>
 (SC-CO<sub>2</sub>
) extraction process of black poplar (Populus nigra L.) buds was optimized (pressure, temperature) based on the yields of major phytochemicals (volatiles and non-volatiles). The optimal settings were 30 MPa/60 °C. Major volatiles determined by GC-MS in the optimized SC-CO<sub>2</sub>
 extract (mg of benzyl salicylate equivalent (BSE) per 100 g of buds) were: pinostrobin chalcone (1574.2), β-eudesmol (640.8), α-eudesmol (581.9), 2-methyl-2-butenyl-p-coumarate (289.9), pentyl-p-coumarate (457.0), γ-eudesmol (294.4), and benzyl salicylate (289.2). Partial qualitative similarity was observed between SC-CO<sub>2</sub>
 extracts and corresponding hydrodistilled essential oil dominated by sesquiterpenes, but with lower yields. Major compounds (mg per 100 g of buds) identified by UHPLC-DAD-QqTOF-MS in the optimized SC-CO<sub>2</sub>
 extract were: pinostrobin (751.7), pinocembrin (485.6), 3-O-pinobanksin acetate and methyl-butenyl-p-coumarate (290.2; 144.9 of pinobanksin and p-coumaric acid equivalents, respectively). SC-CO<sub>2</sub>
 extraction was found useful for green, efficient and simultaneous extraction of both volatile/non-volatile, bioactive phytochemicals of poplar buds - precursors of poplar-type propolis.</AbstractText>
<CopyrightInformation>Copyright © 2018 Elsevier B.V. All rights reserved.</CopyrightInformation>
</Abstract>
<AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Kuś</LastName>
<ForeName>Piotr M</ForeName>
<Initials>PM</Initials>
<AffiliationInfo><Affiliation>Department of Pharmacognosy, Wrocław Medical University, ul. Borowska 211a, 50-556, Wrocław, Poland. Electronic address: piotr.kus@umed.wroc.pl.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Okińczyc</LastName>
<ForeName>Piotr</ForeName>
<Initials>P</Initials>
<AffiliationInfo><Affiliation>Department of Pharmacognosy, Wrocław Medical University, ul. Borowska 211a, 50-556, Wrocław, Poland. Electronic address: piotrokinczyc@gmail.com.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Jakovljević</LastName>
<ForeName>Martina</ForeName>
<Initials>M</Initials>
<AffiliationInfo><Affiliation>Faculty of Food Technology, Josip Juraj Strossmayer University of Osijek, Franje Kuhača 20, 31000, Osijek, Croatia. Electronic address: mjakovljevic@ptfos.hr.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Jokić</LastName>
<ForeName>Stela</ForeName>
<Initials>S</Initials>
<AffiliationInfo><Affiliation>Faculty of Food Technology, Josip Juraj Strossmayer University of Osijek, Franje Kuhača 20, 31000, Osijek, Croatia. Electronic address: stela.jokic@ptfos.hr.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Jerković</LastName>
<ForeName>Igor</ForeName>
<Initials>I</Initials>
<AffiliationInfo><Affiliation>Department of Organic Chemistry, Faculty of Chemistry and Technology, University of Split, R. Boškovića 35, 21000, Split, Croatia. Electronic address: igor@ktf-split.hr.</Affiliation>
</AffiliationInfo>
</Author>
</AuthorList>
<Language>eng</Language>
<PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType>
</PublicationTypeList>
<ArticleDate DateType="Electronic"><Year>2018</Year>
<Month>05</Month>
<Day>25</Day>
</ArticleDate>
</Article>
<MedlineJournalInfo><Country>England</Country>
<MedlineTA>J Pharm Biomed Anal</MedlineTA>
<NlmUniqueID>8309336</NlmUniqueID>
<ISSNLinking>0731-7085</ISSNLinking>
</MedlineJournalInfo>
<ChemicalList><Chemical><RegistryNumber>0</RegistryNumber>
<NameOfSubstance UI="D005419">Flavonoids</NameOfSubstance>
</Chemical>
<Chemical><RegistryNumber>0</RegistryNumber>
<NameOfSubstance UI="D010936">Plant Extracts</NameOfSubstance>
</Chemical>
<Chemical><RegistryNumber>0</RegistryNumber>
<NameOfSubstance UI="D012717">Sesquiterpenes</NameOfSubstance>
</Chemical>
<Chemical><RegistryNumber>142M471B3J</RegistryNumber>
<NameOfSubstance UI="D002245">Carbon Dioxide</NameOfSubstance>
</Chemical>
</ChemicalList>
<CitationSubset>IM</CitationSubset>
<MeshHeadingList><MeshHeading><DescriptorName UI="D002245" MajorTopicYN="N">Carbon Dioxide</DescriptorName>
<QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName>
</MeshHeading>
<MeshHeading><DescriptorName UI="D005591" MajorTopicYN="N">Chemical Fractionation</DescriptorName>
<QualifierName UI="Q000295" MajorTopicYN="N">instrumentation</QualifierName>
<QualifierName UI="Q000379" MajorTopicYN="Y">methods</QualifierName>
</MeshHeading>
<MeshHeading><DescriptorName UI="D002851" MajorTopicYN="N">Chromatography, High Pressure Liquid</DescriptorName>
<QualifierName UI="Q000295" MajorTopicYN="N">instrumentation</QualifierName>
<QualifierName UI="Q000379" MajorTopicYN="N">methods</QualifierName>
</MeshHeading>
<MeshHeading><DescriptorName UI="D005419" MajorTopicYN="N">Flavonoids</DescriptorName>
<QualifierName UI="Q000302" MajorTopicYN="N">isolation & purification</QualifierName>
<QualifierName UI="Q000494" MajorTopicYN="N">pharmacology</QualifierName>
</MeshHeading>
<MeshHeading><DescriptorName UI="D008401" MajorTopicYN="N">Gas Chromatography-Mass Spectrometry</DescriptorName>
<QualifierName UI="Q000295" MajorTopicYN="N">instrumentation</QualifierName>
<QualifierName UI="Q000379" MajorTopicYN="N">methods</QualifierName>
</MeshHeading>
<MeshHeading><DescriptorName UI="D055772" MajorTopicYN="N">Green Chemistry Technology</DescriptorName>
<QualifierName UI="Q000295" MajorTopicYN="N">instrumentation</QualifierName>
<QualifierName UI="Q000379" MajorTopicYN="Y">methods</QualifierName>
</MeshHeading>
<MeshHeading><DescriptorName UI="D010936" MajorTopicYN="N">Plant Extracts</DescriptorName>
<QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName>
<QualifierName UI="Q000494" MajorTopicYN="N">pharmacology</QualifierName>
</MeshHeading>
<MeshHeading><DescriptorName UI="D032107" MajorTopicYN="N">Populus</DescriptorName>
<QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName>
</MeshHeading>
<MeshHeading><DescriptorName UI="D012717" MajorTopicYN="N">Sesquiterpenes</DescriptorName>
<QualifierName UI="Q000302" MajorTopicYN="N">isolation & purification</QualifierName>
<QualifierName UI="Q000494" MajorTopicYN="N">pharmacology</QualifierName>
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<MeshHeading><DescriptorName UI="D013696" MajorTopicYN="N">Temperature</DescriptorName>
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<KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">Central composite design</Keyword>
<Keyword MajorTopicYN="N">Phenolics</Keyword>
<Keyword MajorTopicYN="N">Response surface methodology</Keyword>
<Keyword MajorTopicYN="N">Sesquiterpenes</Keyword>
<Keyword MajorTopicYN="N">Supercritical CO(2) extraction</Keyword>
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<PubmedData><History><PubMedPubDate PubStatus="received"><Year>2018</Year>
<Month>04</Month>
<Day>09</Day>
</PubMedPubDate>
<PubMedPubDate PubStatus="revised"><Year>2018</Year>
<Month>05</Month>
<Day>22</Day>
</PubMedPubDate>
<PubMedPubDate PubStatus="accepted"><Year>2018</Year>
<Month>05</Month>
<Day>23</Day>
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<PubMedPubDate PubStatus="pubmed"><Year>2018</Year>
<Month>6</Month>
<Day>1</Day>
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<PubMedPubDate PubStatus="medline"><Year>2018</Year>
<Month>11</Month>
<Day>6</Day>
<Hour>6</Hour>
<Minute>0</Minute>
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<PubMedPubDate PubStatus="entrez"><Year>2018</Year>
<Month>6</Month>
<Day>1</Day>
<Hour>6</Hour>
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<PublicationStatus>ppublish</PublicationStatus>
<ArticleIdList><ArticleId IdType="pubmed">29852355</ArticleId>
<ArticleId IdType="pii">S0731-7085(18)30809-4</ArticleId>
<ArticleId IdType="doi">10.1016/j.jpba.2018.05.041</ArticleId>
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</PubmedData>
</pubmed>
<affiliations><list><country><li>Croatie</li>
<li>Pologne</li>
</country>
</list>
<tree><country name="Pologne"><noRegion><name sortKey="Ku, Piotr M" sort="Ku, Piotr M" uniqKey="Ku P" first="Piotr M" last="Ku">Piotr M. Ku</name>
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<name sortKey="Oki Czyc, Piotr" sort="Oki Czyc, Piotr" uniqKey="Oki Czyc P" first="Piotr" last="Oki Czyc">Piotr Oki Czyc</name>
</country>
<country name="Croatie"><noRegion><name sortKey="Jakovljevi, Martina" sort="Jakovljevi, Martina" uniqKey="Jakovljevi M" first="Martina" last="Jakovljevi">Martina Jakovljevi</name>
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<name sortKey="Jerkovi, Igor" sort="Jerkovi, Igor" uniqKey="Jerkovi I" first="Igor" last="Jerkovi">Igor Jerkovi</name>
<name sortKey="Joki, Stela" sort="Joki, Stela" uniqKey="Joki S" first="Stela" last="Joki">Stela Joki</name>
</country>
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Development of supercritical CO2 extraction of bioactive phytochemicals from black poplar (Populus nigra L.) buds followed by GC-MS and UHPLC-DAD-QqTOF-MS.

Development of supercritical CO2 extraction of bioactive phytochemicals from black poplar (Populus nigra L.) buds followed by GC-MS and UHPLC-DAD-QqTOF-MS.

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